Superplasticidad de aceros de baja aleación con grano ultrafino
Superplasticity of ultrafine grained low-alloy steels
Keywords:
Superplasticity, Ultrafine grained, Strain rate m coefficient, Boundary sliding, Highstrength low alloy steels (HSLA steels)Abstract
Write Steels with ultrafine grained structure may present superplastic behavior at specific temperatures and strain rates that allow the grain boundary sliding mechanisms to be activated. The superplastic behavior implies deformation to large strains by grain-boundary sliding with diffusional accommodation, as described by the Ashby-Verrall model. The work presents high temperature tension tests in a low carbon, low alloy steel obtained by advanced thermomechanical controlled rolling processes, showing at 800°C elongations as high as 200%.
The microstructure of the steel was analyzed in order to identify ferrite and pearlite grain boundaries, and their interaction after the specimens were deformed. Microanalytical techniques (Optical and SEM) show evidence of: damage growth that prevents the development of higher elongations to failure, non-uniform flow (relative movement-rotation of grains in close proximity to each other) and intergranular non-superplastic deformation (quasi-uniform flow); thus leading to premature failure.
Downloads
References
[2] Sherby, O.D.; Wadsworth, J. and Oyama, T. Superplasticity: Prerequisites and Phenomenology. U.P. Madrid. Madrid : s.n., 1985. E.T.S.I.C.C.P.
[3] Alden, T.H. Plastic deformation of materials. Review Topics in Superplasticity, NY Academic Press, NY, USA, 1975, pp. 225-266.
[4] González, R., García, J.O., Barbés, M.A., Quintana, M.J., Verdeja, L.F., Verdeja, J.I. Ultrafine Grained HSLA Steels for Cold Forming. J Iron Steel Research Int, 2010, vol. 17, num. 10, pp. 50-56.
[5] Avery, D.H. and Backofen, W.A. Trans ASM, 1965, vol. 58, pp. 551-562.
[6] Ashby, M.F. and Verrall, R.A. Diffusion-accomodated flow and superplasticity, Acta Metall Mater, 1973, vol. 21, p. 149.
[7] Pero-Sanz, J.A. Science and Materials Engineering, CIE–Dossat 2000, Madrid, Spain, 2006, pp.
[8] Projects: ULSAB, http://www.ulsab.org/Projects/ULSAB.aspx, (2012).
[9] Mukherjee, K.; Hazra, S.S. and Militzer, M. Grain refinement in dual-phase steels, Met and Mat Trans A, 2009, vol. 40A, pp. 2145-2159.
[10] Quintana, M.J., Gonzalez, R.; Verdeja, L.F. and Verdeja, J.I. Dual-Phase Ultrafine-Grained Steels Produced by Controlled Rolling Processes, Materials Science and Technology (MS&T) 2011, Ohio, USA, 2011, p. 504
[11] Howe, A.A. Ultrafine grained steels: industrial prospects, Mater Sci Tech Ser, 2000, vol. 16, pp. 1264-1266.
[12] Gonzalez, R.; Quintana, M.J.; Verdeja, L.F. and Verdeja, J.I. Ultrafine grained steels and the n coefficient of strain hardening, Memoria de Trabajos de Difusion Cientifica y Tecnica, 2011, vol. 9, pp. 45-54.
[13] Backofen, W. A.; Turner I. R. and Avery, H. Superplasticity in an Al-Zn Alloy, Trans ASM, 1964, vol. 57, pp. 980-990.
[14] Backofen, W. A. Deformation processing, Met Trans., 1973, vol. 4, pp. 2679–2699.
[15] Baudelet, B. La Superplasticite et la mise en Forme des materiaux, Memoires Scientifiques Revue Metalurgie, 1971, vol. 68, pp. 479-487.
[16] Morrison, W.B. Superplasticity of Low-Alloy Steels, Trans ASM, 61 (1968), 423-434.
[17] Reed–Hill, R.E. Creep. Physical Metallurgy Principles, Cengage Learning, Independence, KY, 2nd ed., 1994, pp. 827–887.
[18] Vetrano, J.S. Superplasticity: Mechanisms and applications, JOM, 2001, vol. 3, p. 22.
[19] Pero-Sanz, J. A. Steels: Physical Metallurgy. Selection and Design, CIE–Dossat 2000, Madrid, Spain, 2004. (in Spanish)
[20] Furuhara, T. and Maki, T. Grain boundary engineering for superplasticity in steels, J Mater Sci, 2005, vol. 40, pp. 919-926.
[21] Davies, G.J.; Edington, J.W.; Cutler, C.P. and Padmanabhan, K.A. Superplasticity: A Review, J Mater Sci, 1970, vol. 5, pp. 1091-1102.
[22] Porter, D.A. and Easterling, K.E. Phase Transformations in Metals and Alloys, Chapman & Hall, London, UK, 2nd ed., 1996.
[23] Frommeyer, G. and Jiménez, J.A. Structural Superplasticity at Higher Strain Rates of Hypereutectoid Fe-5.5Al-1Sn-1Cr-1.3C Steel, Met and Mat Trans A, 2005, vol. 36A, pp. 295-300.
[24] Vervynckt, S.; Verbeken, K.; López, B. and Jona, J.J. Modern HSLA steel and role of non – recrystallisation temperature, International Materials Review, 2012, vol. 57, pp. 187-207.
[25] Pero-Sanz, J.A.; Sancho, J.P.; Verdeja, J.I. and L.F. Verdeja, Ferritic grain size: an ignored factor, in fact, in the failure analysis of the sinking of a famous ship, DYNA, 2012, vol. 174, pp. 156-161.